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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">powder</journal-id><journal-title-group><journal-title xml:lang="ru">Известия вузов. Порошковая металлургия и функциональные покрытия</journal-title><trans-title-group xml:lang="en"><trans-title>Powder Metallurgy аnd Functional Coatings (Izvestiya Vuzov. Poroshkovaya Metallurgiya i Funktsional'nye Pokrytiya)</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">1997-308X</issn><issn pub-type="epub">2412-8767</issn><publisher><publisher-name>НИТУ "МИСИС"</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.17073/1997-308X-2025-4-28-39</article-id><article-id custom-type="elpub" pub-id-type="custom">powder-1014</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>Теория и процессы формования и спекания порошковых материалов</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>Theory and Processes of Formation and Sintering of Powder Materials</subject></subj-group></article-categories><title-group><article-title>Особенности уплотнения, формирования структуры и свойств порошкового титана при горячей штамповке</article-title><trans-title-group xml:lang="en"><trans-title>Features of densification, structure formation, and properties of powder titanium under hot die forging</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0001-6743-1727</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Дорофеев</surname><given-names>В. Ю.</given-names></name><name name-style="western" xml:lang="en"><surname>Dorofeyev</surname><given-names>V. Yu.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Владимир Юрьевич Дорофеев – д.т.н., профессор кафедры «Материаловедение и технология машиностроения»</p><p>Россия, 346428, Ростовская обл., г. Новочеркасск, ул. Просвещения, 132</p></bio><bio xml:lang="en"><p>Vladimir Yu. Dorofeyev – Dr. Sci. (Eng.), Professor of the Department of material science and engineering technology</p><p>132 Prosveshcheniya Str., Rostov region, Novocherkassk 346428, Russia</p></bio><email xlink:type="simple">dvyu56.56@mail.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0002-9851-1073</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Свиридова</surname><given-names>А. Н.</given-names></name><name name-style="western" xml:lang="en"><surname>Sviridova</surname><given-names>A. N.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Анна Николаевна Свиридова – к.т.н., доцент кафедры «Автомобили и транспортно-технологические комплексы»</p><p>Россия, 346428, Ростовская обл., г. Новочеркасск, ул. Просвещения, 132</p></bio><bio xml:lang="en"><p>Anna N. Sviridova – Cand. Sci. (Eng.), Associate Prof. of the Department of Automobiles and Transport-Technological Complexes</p><p>132 Prosveshcheniya Str., Rostov region, Novocherkassk 346428, Russia</p></bio><email xlink:type="simple">anysviridova@yandex.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0009-0007-5260-3726</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Свиридова</surname><given-names>С. В.</given-names></name><name name-style="western" xml:lang="en"><surname>Sviridova</surname><given-names>S. V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Светлана Владимировна Свиридова – ординатор института медицины и здоровьесбережения</p><p>Россия, 392000, г. Тамбов, ул. Интернациональная, 33</p></bio><bio xml:lang="en"><p>Svetlana V. Sviridova – Resident of the Institute of Medicine and Health Preservation</p><p>33 Internatsionalnaya Str., Tambov 392000, Russia</p></bio><email xlink:type="simple">dr.sviridova27@inbox.ru</email><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0009-0001-8552-2582</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Свистун</surname><given-names>Л. И.</given-names></name><name name-style="western" xml:lang="en"><surname>Svistun</surname><given-names>L. I.</given-names></name></name-alternatives><bio xml:lang="ru"><p>Лев Иванович Свистун – д.т.н., профессор кафедры инженерии систем управления, материалов и технологий в машиностроении</p><p>Россия, 350072, г. Краснодар, ул. Московская, 2</p></bio><bio xml:lang="en"><p>Lev I. Svistun – Dr. Sci. (Eng.), Professor of the Department of Engineering of Control Systems, Materials and Technologies in Mechanical Engineering</p><p>2 Moskovskaya Str., Krasnodar 350072, Russia</p></bio><email xlink:type="simple">levsvistun45@gmail.com</email><xref ref-type="aff" rid="aff-3"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Южно-Российский государственный политехнический университет (НПИ) имени М.И. Платова</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Platov South-Russian State Polytechnic University (NPI)</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Тамбовский государственный университет имени Г.Р. Державина</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Tambov State University named after G.R. Derzhavin</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru"><institution>Кубанский государственный технологический университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Kuban State Technological University</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2025</year></pub-date><pub-date pub-type="epub"><day>30</day><month>08</month><year>2025</year></pub-date><volume>19</volume><issue>4</issue><fpage>28</fpage><lpage>39</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; НИТУ "МИСИС", 2025</copyright-statement><copyright-year>2025</copyright-year><copyright-holder xml:lang="ru">НИТУ "МИСИС"</copyright-holder><copyright-holder xml:lang="en">НИТУ "МИСИС"</copyright-holder><license xlink:href="https://powder.misis.ru/jour/about/submissions#copyrightNotice" xlink:type="simple"><license-p>https://powder.misis.ru/jour/about/submissions#copyrightNotice</license-p></license></permissions><self-uri xlink:href="https://powder.misis.ru/jour/article/view/1014">https://powder.misis.ru/jour/article/view/1014</self-uri><abstract><p>Работы в области порошковой металлургии титана проводятся уже более 60 лет. Несмотря на это, примеров практического использования порошкового титана не так много, что связано с неудовлетворительным характером показателей надежности и долговечности получаемых изделий. Способность титановых изделий сопротивляться воздействию статических и динамических нагрузок определяется наличием остаточной пористости, неметаллических включений, а также характеристиками микроструктуры. В настоящее время при изготовлении изделий из порошкового титана наибольшее распространение получила технология прессования–спекания. Однако пористость спеченного титана составляет 3–15 %, что снижает его сопротивляемость действию нагрузок и обусловливает актуальность разработки эффективных методов снижения пористости. Большой потенциал в решении указанной задачи имеют методы горячей обработки давлением, в частности горячая штамповка пористых заготовок. В работе представлены результаты исследования особенностей уплотнения, формирования структуры и свойств порошкового титана при горячей штамповке. Предложена технология получения горячештампованного порошкового титана, включающая выполнение операций гидрирования–дегидрирования пористой заготовки, обеспечивающих восстановление оксидов, локализованных на поверхностях открытых пор, водородом и их активизацию, что способствует улучшению условий формирования межчастичного сращивания при последующей горячей допрессовке и повышению трещиностойкости и пластичности получаемых образцов в сравнении с образцами-свидетелями. Установлены значения величины максимальной приведенной работы горячего уплотнения пористого порошкового титана, необходимой для достижения плотности монолита, при разных температурах преддеформационного нагрева заготовок. Показано, что немонотонность температурной зависимости максимальной приведенной работы уплотнения связана с формированием крупнозернистой структуры и с уменьшением пластичности деформируемого материала в интервале температур фазового α → β-превращения.</p></abstract><trans-abstract xml:lang="en"><p>Research in the field of titanium powder metallurgy has been ongoing for more than 60 years. Nevertheless, there are relatively few examples of the practical application of powder titanium, which is associated with insufficient reliability and durability of the manufactured products. The ability of titanium parts to withstand static and dynamic loads is determined by residual porosity, non-metallic inclusions, and microstructural characteristics. At present, the most widely used method for producing powder titanium components is the press–sinter route. However, the porosity of sintered titanium typically ranges from 3 to 15 %, which reduces its load-bearing capacity and highlights the need for effective methods to minimize porosity. Hot working methods, particularly hot die forging of porous preforms, hold considerable potential in addressing this issue. This study presents the results of investigating the features of densification, structure formation, and properties of powder titanium under hot die forging. A technology for producing hot-forged powder titanium is proposed, which includes hydriding–dehydriding of porous preforms. This operation promotes the reduction of oxides localized on the surfaces of open pores by hydrogen and their activation, thereby improving conditions for interparticle bonding during subsequent hot repressing. As a result, the obtained samples demonstrate higher fracture toughness and ductility compared with reference samples. The values of the maximum specific work of hot densification of porous powder titanium, required to achieve monolithic density at different preheating temperatures of the preforms, were determined. It was shown that the non-monotonic temperature dependence of the maximum specific densification work is associated with the formation of a coarse-grained structure and with reduced ductility of the deformable material in the temperature range of the α → β phase transformation.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>горячая штамповка</kwd><kwd>пористые заготовки</kwd><kwd>порошковый титан</kwd><kwd>работа уплотнения</kwd><kwd>трещиностойкость</kwd><kwd>пластичность</kwd><kwd>прочность</kwd><kwd>вязкий излом</kwd><kwd>межчастичное разрушение</kwd><kwd>восстановление оксидов</kwd><kwd>гидрирование</kwd><kwd>дегидрирование</kwd><kwd>межчастичное сращивание</kwd><kwd>активация</kwd></kwd-group><kwd-group xml:lang="en"><kwd>hot die forging</kwd><kwd>porous preforms</kwd><kwd>powder titanium</kwd><kwd>densification work</kwd><kwd>fracture toughness</kwd><kwd>ductility</kwd><kwd>strength</kwd><kwd>ductile fracture</kwd><kwd>interparticle fracture</kwd><kwd>oxide reduction</kwd><kwd>hydriding</kwd><kwd>dehydriding</kwd><kwd>interparticle bonding</kwd><kwd>activation</kwd></kwd-group><funding-group><funding-statement xml:lang="ru">Снимки на растровом микроскопе-микроанализаторе Quanta 200 i 3D получены в Центре коллективного пользования «Нанотехнологии» ЮРГПУ (НПИ). Авторы выражают благодарность компании «Хёганес Восточная Европа» за предос­тавленный железный порошок ABC100.30 производства фирмы Höganäs AB.</funding-statement><funding-statement xml:lang="en">The SEM images were obtained using a Quanta 200 i 3D microanalyzer at the Nanotechnology Shared Research Facility of Platov South-Russian State Polytechnic University. The authors express their gratitude to Höganäs Eastern Europe for providing the ABC100.30 iron powder manufactured by Höganäs AB.</funding-statement></funding-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Fang Z.Z., Paramore J.D., Sun P., Chandrana K.S.R., Zhang Y., Xia Y., Cao F., Koopman M.M., Free M.M. Powder metallurgy of titanium – past, present, and future. 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